5K93
PapD wild-type chaperone
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | NSLS BEAMLINE X29A |
| Synchrotron site | NSLS |
| Beamline | X29A |
| Temperature [K] | 277.15 |
| Detector technology | CCD |
| Collection date | 2014-08-07 |
| Detector | ADSC QUANTUM 315 |
| Wavelength(s) | 1.0749 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 83.129, 70.989, 93.050 |
| Unit cell angles | 90.00, 102.05, 90.00 |
Refinement procedure
| Resolution | 49.190 - 2.700 |
| R-factor | 0.22342 |
| Rwork | 0.220 |
| R-free | 0.27858 |
| RMSD bond length | 0.012 |
| RMSD bond angle | 1.600 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | PHENIX |
| Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 49.200 |
| High resolution limit [Å] | 2.700 |
| Number of reflections | 13917 |
| <I/σ(I)> | 23.6 |
| Completeness [%] | 96.8 |
| Redundancy | 3.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 277.15 | 0.1 M citric acid, pH 3.6, 25% PEG-3350 |
