5K8J
Structure of Caulobacter crescentus VapBC1 (apo form)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | MAX II BEAMLINE I911-3 |
Synchrotron site | MAX II |
Beamline | I911-3 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-04-30 |
Detector | MARMOSAIC 225 mm CCD |
Wavelength(s) | 0.972 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 86.290, 86.290, 113.820 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 37.400 - 1.600 |
R-factor | 0.1582 |
Rwork | 0.158 |
R-free | 0.16810 |
Structure solution method | SAD |
RMSD bond length | 0.014 |
RMSD bond angle | 1.134 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((1.10_2152: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 37.400 | 1.640 |
High resolution limit [Å] | 1.600 | 1.600 |
Number of reflections | 125126 | |
<I/σ(I)> | 22.8 | 1.7 |
Completeness [%] | 100.0 | 100 |
Redundancy | 23.2 | 22.8 |
CC(1/2) | 1.000 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.5 | 292.15 | 3 M NaCl, 0.1 M Bis-tris pH 5.5, 5 mM MgCl2, 5 mM beta-mercapto ethanol, 25% glycerol |