5K7S

MicroED structure of proteinase K at 1.6 A resolution

Experimental procedure

Spacegroup name	P 43 21 2
Unit cell lengths	67.059, 67.059, 100.713
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	20.751 - 1.600
R-factor	0.2255
Rwork	0.224
R-free	0.25460
RMSD bond length	0.004
RMSD bond angle	0.633
Refinement software	PHENIX ((1.10_2155: ???))

Data quality characteristics

	Overall	Inner shell	Outer shell
Low resolution limit [Å]	20.750	20.750	1.320
High resolution limit [Å]	1.300	7.120	1.300
Rmerge	0.728	0.200	2.455
Rpim	0.295	0.073	1.984
Number of reflections	46369	386	1005
<I/σ(I)>	2.4	8.1	0.4
Completeness [%]	81.1	93.1	36.6
Redundancy	6.5	7.1	2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1