5K6W
Sidekick-1 immunoglobulin domains 1-5
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X4C |
Synchrotron site | NSLS |
Beamline | X4C |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-05-04 |
Detector | MAR CCD 165 mm |
Wavelength(s) | 0.979 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 70.140, 152.870, 158.970 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 36.997 - 3.500 |
R-factor | 0.2044 |
Rwork | 0.202 |
R-free | 0.25100 |
RMSD bond length | 0.003 |
RMSD bond angle | 0.613 |
Data reduction software | iMOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((1.10.1_2155: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 3.670 |
High resolution limit [Å] | 3.500 | 3.500 |
Rmerge | 0.132 | 0.304 |
Number of reflections | 19853 | |
<I/σ(I)> | 9.9 | 3.9 |
Completeness [%] | 89.9 | 79.5 |
Redundancy | 3.3 | 2.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | BATCH MODE | 295 | 1.4M ammonium sulfate, 0.5M lithium chloride, 10mM yttrium chloride |