Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ALS BEAMLINE 8.3.1 |
| Synchrotron site | ALS |
| Beamline | 8.3.1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2011-12-20 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 1 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 150.240, 55.880, 101.620 |
| Unit cell angles | 90.00, 110.50, 90.00 |
Refinement procedure
| Resolution | 48.974 - 3.090 |
| R-factor | 0.2089 |
| Rwork | 0.202 |
| R-free | 0.27490 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 4rs8 |
| RMSD bond length | 0.002 |
| RMSD bond angle | 0.714 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | MOLREP |
| Refinement software | PHENIX (1.6.4_486) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 48.974 | 3.200 |
| High resolution limit [Å] | 3.090 | 3.090 |
| Number of reflections | 14275 | |
| <I/σ(I)> | 6 | 2.3 |
| Completeness [%] | 96.7 | |
| Redundancy | 4 | 2.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 298 | PEG 200, phosphate/citrate |
