Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ALS BEAMLINE 8.3.1 |
| Synchrotron site | ALS |
| Beamline | 8.3.1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2011-11-19 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 1 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 102.400, 62.000, 62.000 |
| Unit cell angles | 90.00, 109.70, 90.00 |
Refinement procedure
| Resolution | 58.371 - 2.825 |
| R-factor | 0.2363 |
| Rwork | 0.232 |
| R-free | 0.27620 |
| Structure solution method | SAD |
| RMSD bond length | 0.003 |
| RMSD bond angle | 0.532 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.6.4_486) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 58.371 | |
| High resolution limit [Å] | 2.825 | 2.825 |
| Rmerge | 0.099 | 0.490 |
| Number of reflections | 17036 | |
| <I/σ(I)> | 9 | 1.9 |
| Completeness [%] | 99.1 | |
| Redundancy | 3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 298 | PEG 3350, citrate |
