5JZV
The structure of D77G hCINAP-ADP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | BSRF BEAMLINE 3W1A |
Synchrotron site | BSRF |
Beamline | 3W1A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-06-15 |
Detector | MAR CCD 130 mm |
Wavelength(s) | 0.9792 |
Spacegroup name | P 61 |
Unit cell lengths | 101.757, 101.757, 58.854 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 44.060 - 2.070 |
R-factor | 0.192 |
Rwork | 0.190 |
R-free | 0.23500 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3iil |
RMSD bond length | 0.033 |
RMSD bond angle | 2.023 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.5.0110) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.140 |
High resolution limit [Å] | 2.070 | 2.070 |
Number of reflections | 21343 | |
<I/σ(I)> | 50.2 | |
Completeness [%] | 100.0 | 100 |
Redundancy | 22.9 | 21.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.6 | 293 | 0.01M MAGNESIUM CHLORIDE HEXAHYDRATE, 0.05M MES MONOHYDRATE PH 5.6, 1.8M LITHIUM SULFATE MONOHYDRATE, VAPOR DIFFUSION, SITTING DROP, TEMPERATURE 293K |