5JYS
Pry1 CAP domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E+ SUPERBRIGHT |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2015-11-25 |
Detector | RIGAKU |
Wavelength(s) | 1.514 |
Spacegroup name | I 41 |
Unit cell lengths | 69.105, 69.105, 97.730 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 34.553 - 1.901 |
R-factor | 0.1985 |
Rwork | 0.198 |
R-free | 0.20830 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5ete |
RMSD bond length | 0.003 |
RMSD bond angle | 0.533 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASES |
Refinement software | PHENIX ((dev_2405)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 34.553 | 1.990 |
High resolution limit [Å] | 1.890 | 1.890 |
Rmerge | 0.082 | 0.428 |
Number of reflections | 18355 | |
<I/σ(I)> | 9.4 | 2.3 |
Completeness [%] | 100.0 | 100 |
Redundancy | 3.6 | 3.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 298 | 100mM Tris pH 8.5, 0.2M Magnesium chloride |