5JYN
Structure of the transmembrane domain of HIV-1 gp41 in bicelle
Spectrometer
Experimental method: SOLUTION NMR
| Spectrometer ID | Spectrometer maker | Spectrometer model | Spectrometer type | Spectrometer field strength |
| 1 | Bruker | AVANCE II | 600 | |
| 2 | Bruker | AVANCE II | 750 | |
| 3 | Bruker | AVANCE III | 900 |
Experiment
| experiment id | conditions id | solution id | Experiment type |
| 1 | 1 | 1 | 3D TROSY HNCA |
| 2 | 1 | 1 | 3D TROSY HNCOCA |
| 3 | 1 | 1 | 3D TROSY HNCACO |
| 4 | 1 | 1 | 3D TROSY HNCO |
| 5 | 1 | 2 | 3D 15N NOESY-TROSY-HSQC |
| 6 | 1 | 2 | 3D 13C NOESY-HSQC (Methyls) |
| 7 | 1 | 3 | 3D 15N NOESY-TROSY-HSQC (long mixing time) |
| 8 | 1 | 1 | 2D 15N TROSY-HSQC for GdDOTA titration |
| 9 | 1 | 4 | 3D 15N NOESY-TROSY-HSQC (short mixing time) |
NMR Sample
| conditions id | NMR sample pH | NMR sample pressure | NMR sample temperature |
| 1 | 6.7 | 1 | 303 |
Conformers
| Conformers Calculated Total Number | 150 |
| Conformers Submitted Total Number | 15 |
