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5JXK

Crystal structure of Porphyromonas endodontalis DPP11

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsESRF BEAMLINE MASSIF-1
Synchrotron siteESRF
BeamlineMASSIF-1
Temperature [K]100
Detector technologyPIXEL
Collection date2015-08-31
DetectorDECTRIS PILATUS3 2M
Wavelength(s)0.966
Spacegroup nameP 21 21 21
Unit cell lengths76.752, 91.831, 229.917
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution46.697 - 2.850
R-factor0.2417
Rwork0.240
R-free0.27340
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.003
RMSD bond angle0.741
Data reduction softwareXDS
Data scaling softwareSCALA (3.3.20)
Phasing softwarePHASER
Refinement softwarePHENIX
Data quality characteristics
 OverallInner shellOuter shell
Low resolution limit [Å]114.95946.6973.000
High resolution limit [Å]2.8509.0102.850
Rmerge0.0561.118
Rmeas0.2450.0611.213
Rpim0.0940.0240.468
Total number of observations257565887336813
Number of reflections38861
<I/σ(I)>7.526.21.7
Completeness [%]100.099.3100
Redundancy6.66.46.6
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP2930.1 M Tris-HCl pH 7.5, 15 % PEG 6000

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