5JXC
SynGAP Coiled-coil trimer
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-03-24 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.97886 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 28.803, 236.664, 42.207 |
Unit cell angles | 90.00, 96.92, 90.00 |
Refinement procedure
Resolution | 39.497 - 2.500 |
R-factor | 0.2271 |
Rwork | 0.223 |
R-free | 0.30700 |
Structure solution method | MAD |
RMSD bond length | 0.008 |
RMSD bond angle | 0.969 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX (1.10_2155) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.540 |
High resolution limit [Å] | 2.500 | 2.500 |
Number of reflections | 19240 | |
<I/σ(I)> | 22.8 | |
Completeness [%] | 99.7 | |
Redundancy | 3.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 289 | 0.1M HEPES sodium pH 7.5, 0.1M L-proline, 20% w/v Polyethylene glycol 1500 |