5JVM
The neck-linker and alpha 7 helix of Mus musculus KIF3C
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-ID |
Synchrotron site | APS |
Beamline | 19-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-12-13 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.97924 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 72.074, 71.979, 43.142 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 37.004 - 1.567 |
R-factor | 0.1788 |
Rwork | 0.177 |
R-free | 0.20520 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1yib |
RMSD bond length | 0.005 |
RMSD bond angle | 0.644 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHASER |
Refinement software | PHENIX ((1.10.1_2155: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 37.004 | 1.620 |
High resolution limit [Å] | 1.567 | 1.567 |
Rmerge | 0.073 | 0.595 |
Number of reflections | 44738 | |
<I/σ(I)> | 21.7 | 1.6 |
Completeness [%] | 98.0 | |
Redundancy | 7.1 | 3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 9 | 298 | 30% (w/v) pentaerythritol ethoxylate (PEE) 797, 1.5% (w/v) ethylene glycol monoethylether, 400 mM MgCl2, 100 mM bis-tris propane pH 9.0 |