5JVF
Crystal Structure of Apo-FleN
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE BM14 |
Synchrotron site | ESRF |
Beamline | BM14 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-10-04 |
Detector | MAR CCD 165 mm |
Wavelength(s) | 0.95372 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 66.250, 66.250, 112.870 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 25.573 - 1.660 |
R-factor | 0.1901 |
Rwork | 0.189 |
R-free | 0.21710 |
Structure solution method | SAD |
RMSD bond length | 0.007 |
RMSD bond angle | 1.095 |
Data reduction software | iMOSFLM |
Data scaling software | SCALA |
Phasing software | AutoSol |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 28.690 | 1.750 |
High resolution limit [Å] | 1.660 | 1.660 |
Number of reflections | 65124 | |
<I/σ(I)> | 17.6 | |
Completeness [%] | 99.6 | |
Redundancy | 7.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 277 | 0.2M Ammonium iodide, 20% PEG3350 |