5JUH
Crystal structure of C-terminal domain (RV) of MpAFP
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | CLSI BEAMLINE 08ID-1 |
| Synchrotron site | CLSI |
| Beamline | 08ID-1 |
| Temperature [K] | 93 |
| Detector technology | CCD |
| Collection date | 2016-02-12 |
| Detector | RAYONIX MX-300 |
| Wavelength(s) | 0.97949 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 34.960, 43.340, 78.840 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 39.420 - 1.350 |
| R-factor | 0.12795 |
| Rwork | 0.125 |
| R-free | 0.17709 |
| RMSD bond length | 0.029 |
| RMSD bond angle | 2.357 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0135) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 43.350 |
| High resolution limit [Å] | 1.230 |
| Number of reflections | 27687 |
| <I/σ(I)> | 10.5 |
| Completeness [%] | 78.0 |
| Redundancy | 8.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | MICROBATCH | 4.6 | 298 | Calcium chloride, Sodium acetate, PEG 400 |
