5JTT
Crystal structure of GPb in complex with 8a
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | MAX II BEAMLINE I911-2 |
Synchrotron site | MAX II |
Beamline | I911-2 |
Temperature [K] | 293 |
Detector technology | CCD |
Collection date | 2015-09-05 |
Detector | MAR CCD 165 mm |
Wavelength(s) | 1.0403 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 128.600, 128.600, 116.240 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 38.390 - 1.850 |
R-factor | 0.159 |
Rwork | 0.158 |
R-free | 0.18800 |
Structure solution method | FOURIER SYNTHESIS |
RMSD bond length | 0.010 |
RMSD bond angle | 1.319 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | REFMAC |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 38.390 | 1.950 |
High resolution limit [Å] | 1.850 | 1.850 |
Rmerge | 0.069 | 0.428 |
Number of reflections | 82598 | |
<I/σ(I)> | 12.2 | 3.3 |
Completeness [%] | 99.3 | 98.7 |
Redundancy | 3.9 | 3.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | SMALL TUBES | 6.7 | 289 | 10mM BES buffer |