5JQZ
Designed two-ring homotetramer at 3.8A resolution
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.2.2 |
Synchrotron site | ALS |
Beamline | 8.2.2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-05-30 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 70.690, 37.331, 58.716 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 58.716 - 3.830 |
R-factor | 0.433 |
Rwork | 0.428 |
R-free | 0.47850 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.003 |
RMSD bond angle | 0.681 |
Data reduction software | xia2 |
Data scaling software | xia2 |
Phasing software | PHASER |
Refinement software | PHENIX (dev_1616) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 58.720 |
High resolution limit [Å] | 3.830 |
Number of reflections | 1573 |
<I/σ(I)> | 90.7 |
Completeness [%] | 93.9 |
Redundancy | 3.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 295 | 0.2 M Sodium Acetate trihydrate, 0.1 M Tris hydrochloride pH 8.5 and 30 % PEG 4,000 |