5JNO
Crystal structure of the BD1-NTPR complex from BEND3 and PICH
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-10-20 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 1.0 |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 47.280, 47.280, 431.579 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 71.930 - 2.200 |
R-factor | 0.22236 |
Rwork | 0.222 |
R-free | 0.23748 |
Structure solution method | MAD |
RMSD bond length | 0.013 |
RMSD bond angle | 1.587 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | SHELXDE |
Refinement software | REFMAC (5.8.0123) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 71.930 |
High resolution limit [Å] | 2.200 |
Number of reflections | 14907 |
<I/σ(I)> | 8.7 |
Completeness [%] | 99.1 |
Redundancy | 20 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.1 mM HEPES, pH=7.0 1.56 M ammonium sulphate |