5JNN

Crystal structure of abscisic acid receptor PYL2 in complex with Phaseic acid.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ALS BEAMLINE 8.2.2
Synchrotron site	ALS
Beamline	8.2.2
Temperature [K]	80
Detector technology	CCD
Collection date	2013-06-06
Detector	ADSC QUANTUM 315r
Wavelength(s)	1.0
Spacegroup name	P 61 2 2
Unit cell lengths	60.950, 60.950, 255.812
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	52.780 - 2.300
R-factor	0.191
Rwork	0.189
R-free	0.23500
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.008
RMSD bond angle	1.107
Data reduction software	iMOSFLM
Data scaling software	SCALA
Phasing software	PHASER
Refinement software	PHENIX (1.8.1_1168)

Data quality characteristics

	Overall
Low resolution limit [Å]	52.784
High resolution limit [Å]	2.300
Number of reflections	13406
<I/σ(I)>	23.57
Completeness [%]	99.8
Redundancy	2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		277.15	4 M sodium formate