5JKQ
Crystal structure of Plasmodium falciparum Pf3D7_0606800 (PfVFT1)
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRL BEAMLINE BL7-1 |
| Synchrotron site | SSRL |
| Beamline | BL7-1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2015-08-09 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 1.127 |
| Spacegroup name | P 21 21 2 |
| Unit cell lengths | 84.770, 201.430, 77.560 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 61.450 - 2.350 |
| R-factor | 0.2066 |
| Rwork | 0.204 |
| R-free | 0.26090 |
| Structure solution method | SAD |
| RMSD bond length | 0.003 |
| RMSD bond angle | 0.721 |
| Data reduction software | MOSFLM |
| Data scaling software | Aimless |
| Phasing software | SHELX |
| Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 84.770 | 2.420 |
| High resolution limit [Å] | 2.350 | 2.350 |
| Rmerge | 0.125 | 0.546 |
| Number of reflections | 55998 | |
| <I/σ(I)> | 8.6 | 2.3 |
| Completeness [%] | 99.8 | 99.8 |
| Redundancy | 4.3 | 4.3 |
| CC(1/2) | 0.990 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 291 | 0.1 M Bis-Tris:HCl pH 6.5, 2.0 M ammonium sulfate |
