5JI3

HslUV complex

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ALS BEAMLINE 5.0.2
Synchrotron site	ALS
Beamline	5.0.2
Temperature [K]	100
Detector technology	CCD
Collection date	2000-02-22
Detector	ADSC QUANTUM 315
Wavelength(s)	0.97
Spacegroup name	P 3 2 1
Unit cell lengths	169.995, 169.995, 161.317
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	84.997 - 3.000
R-factor	0.2287
Rwork	0.222
R-free	0.25250
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	1g4a
RMSD bond length	0.002
RMSD bond angle	0.494
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	CNS
Refinement software	CNS ((1.10_2155: ???))

Data quality characteristics

	Overall
<I/σ(I)>	2
Completeness [%]	85.7
Redundancy	2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		300	NA