5JHD
Crystal structure of LS10-TCR/M1-HLA-A*02 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 31-ID |
Synchrotron site | APS |
Beamline | 31-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-07-08 |
Detector | RAYONIX MX225HE |
Wavelength(s) | 0.9793 |
Spacegroup name | P 1 |
Unit cell lengths | 49.710, 101.840, 113.550 |
Unit cell angles | 99.38, 92.60, 103.45 |
Refinement procedure
Resolution | 29.051 - 2.460 |
R-factor | 0.2052 |
Rwork | 0.204 |
R-free | 0.22330 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1oga |
RMSD bond length | 0.003 |
RMSD bond angle | 0.621 |
Data reduction software | iMOSFLM |
Data scaling software | SCALA (3.3.22) |
Phasing software | PHASER (2.5.6) |
Refinement software | PHENIX |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 111.609 | 80.917 | 2.590 |
High resolution limit [Å] | 2.460 | 7.780 | 2.460 |
Rmerge | 0.056 | 0.810 | |
Number of reflections | 72668 | ||
<I/σ(I)> | 8.1 | 9.8 | 0.9 |
Completeness [%] | 94.0 | 97.6 | 72 |
Redundancy | 3.9 | 3.9 | 3.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 294 | 10%(W/V) PEG8000, 100mM Tris-Cl, 200mM Magnesium chloirde |