5JFC
NADH-dependent Ferredoxin:NADP Oxidoreductase (NfnI) from Pyrococcus furiosus
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL12-2 |
Synchrotron site | SSRL |
Beamline | BL12-2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-02-05 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.88 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 179.927, 179.927, 80.792 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 47.592 - 1.598 |
R-factor | 0.1475 |
Rwork | 0.147 |
R-free | 0.15920 |
Structure solution method | SAD |
RMSD bond length | 0.010 |
RMSD bond angle | 1.496 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX ((dev_2313: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.630 |
High resolution limit [Å] | 1.589 | 1.590 |
Rmerge | 0.058 | 0.480 |
Number of reflections | 197382 | |
<I/σ(I)> | 29.5 | 4 |
Completeness [%] | 100.0 | 99.9 |
Redundancy | 8.3 | 7.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 295 | 2.5 M Ammonium formate, 0.1 M HEPES pH 7.0 |