5JDD
Crystal structure of I9-I11 tandem from titin (P212121)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-03-01 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.9795 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 42.340, 65.800, 108.390 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 41.830 - 1.530 |
R-factor | 0.1625 |
Rwork | 0.162 |
R-free | 0.19650 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 1.094 |
Data reduction software | iMOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX (1.8_1069) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 41.830 | 1.610 |
High resolution limit [Å] | 1.530 | 1.530 |
Number of reflections | 45488 | |
<I/σ(I)> | 12.6 | |
Completeness [%] | 97.5 | |
Redundancy | 5.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 292 | 0.1 M Bis-Tris Propane pH 8.5, 20% [w/v] PEG 3350, 0.2 M sodium acetate |