5JCY
Spir2-GTBM bound to MyoVa-GTD
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 1 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-02-12 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.979340 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 99.610, 41.220, 108.220 |
Unit cell angles | 90.00, 115.89, 90.00 |
Refinement procedure
Resolution | 44.806 - 1.800 |
R-factor | 0.1533 |
Rwork | 0.151 |
R-free | 0.19130 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4lx1 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.092 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | MOLREP |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 44.810 | 1.860 |
High resolution limit [Å] | 1.760 | 1.760 |
Number of reflections | 39553 | |
<I/σ(I)> | 15.7 | |
Completeness [%] | 99.1 | |
Redundancy | 6.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 290 | 50 mM Hepes, 50 mM MOPS, 10% (w/v) PEG 1000, 10% (w/v) PEG 3350, 10% (v/v) MPD |