5J8Y
Crystal structure of the Scm-SAM and Sfmbt-SAM heterodimer
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-09-02 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1.0 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 49.956, 53.970, 61.455 |
Unit cell angles | 90.00, 109.22, 90.00 |
Refinement procedure
Resolution | 47.170 - 1.980 |
R-factor | 0.2558 |
Rwork | 0.255 |
R-free | 0.27720 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1pk1 |
RMSD bond length | 0.003 |
RMSD bond angle | 0.706 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1678) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.170 | 2.090 |
High resolution limit [Å] | 1.980 | 1.980 |
Rmerge | 0.136 | 0.870 |
Number of reflections | 21180 | |
<I/σ(I)> | 11.21 | 1.91 |
Completeness [%] | 96.9 | 83.18 |
Redundancy | 9.1 | 6.99 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 277.15 | 0.05M Tris/HCl pH 7.5, 4% MPD, 0.2M ammonium acetate, 32.5% PEG3350 |