5J8P
Lys27-linked diubiquitin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-06-04 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9792 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 44.828, 63.411, 52.844 |
Unit cell angles | 90.00, 109.16, 90.00 |
Refinement procedure
Resolution | 31.706 - 1.554 |
R-factor | 0.2368 |
Rwork | 0.234 |
R-free | 0.29460 |
RMSD bond length | 0.012 |
RMSD bond angle | 1.466 |
Refinement software | PHENIX ((1.10.1_2155: ???)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 31.706 |
High resolution limit [Å] | 1.554 |
Number of reflections | 13686 |
<I/σ(I)> | 13.2 |
Completeness [%] | 67.9 |
Redundancy | 3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 291 | 0.2M magnesium acetate tetrahydrate, 0.1M sodium cacodylate trihydrate, pH 6.5, 20% PEG 8000 |