5J7E
hEAG PAS domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 277 |
Detector technology | CCD |
Collection date | 2009-12-16 |
Detector | MARMOSAIC 225 mm CCD |
Wavelength(s) | 0.9796 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 213.974, 39.058, 106.802 |
Unit cell angles | 90.00, 118.03, 90.00 |
Refinement procedure
Resolution | 29.130 - 1.900 |
R-factor | 0.214 |
Rwork | 0.214 |
R-free | 0.23100 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2z6c |
RMSD bond length | 0.005 |
RMSD bond angle | 1.200 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | CNS (1.2) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.973 |
High resolution limit [Å] | 1.900 | 1.905 |
Number of reflections | 59648 | |
<I/σ(I)> | 4.14 | |
Completeness [%] | 96.4 | |
Redundancy | 1.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 291 | 20 mM Tris-HCl, 200 mM NaCl, 5 mM DTT |