5J1L

Crystal structure of Csd1-Csd2 dimer I

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PAL/PLS BEAMLINE 7A (6B, 6C1)
Synchrotron site	PAL/PLS
Beamline	7A (6B, 6C1)
Temperature [K]	100
Detector technology	CCD
Collection date	2015-10-04
Detector	ADSC QUANTUM 270
Wavelength(s)	0.9793
Spacegroup name	P 1 21 1
Unit cell lengths	53.359, 82.375, 76.290
Unit cell angles	90.00, 106.03, 90.00

Refinement procedure

Resolution	50.010 - 2.270
R-factor	0.17736
Rwork	0.174
R-free	0.23264
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.010
RMSD bond angle	1.466
Data scaling software	HKL-2000
Phasing software	MOLREP
Refinement software	REFMAC (5.8.0123)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.010	2.310
High resolution limit [Å]	2.270	2.270
Number of reflections	29291
<I/σ(I)>	20.8	4
Completeness [%]	99.8	100
Redundancy	4.1	4.1

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		296	HEPES, Jeffamine ED-2001