5J17

Solution structure of Ras Binding Domain (RBD) of B-Raf

Spectrometer

Experimental method: SOLUTION NMR

Spectrometer ID	Spectrometer maker	Spectrometer model	Spectrometer type	Spectrometer field strength
1	Bruker	AVANCE		600
2	Bruker	AVANCE		700
3	Bruker	AVANCE		800
4	Bruker	AVANCE		900

Experiment

experiment id	conditions id	solution id	Experiment type
1	1	1	2D 1H-15N HSQC
10	1	2	3D 1H-15N NOESY
11	1	2	3D HNCACB
12	1	2	3D CBCA(CO)NH
13	1	2	3D HN(CO)CA
2	1	2	2D 1H-13C HSQC
3	1	2	3D HNCO
4	1	2	3D Hn(CA)CO
5	1	2	3D HNCA
6	1	2	3D HCCH-TOCSY
7	1	2	3D H(CCO)NH
8	1	2	3D 1H-13C NOESY aromatic
9	1	2	3D 1H-13C NOESY aliphatic

NMR Sample

conditions id	NMR sample pH	NMR sample pressure	NMR sample temperature
1	7.4	1	298

Conformers

Conformers Calculated Total Number	1024
Conformers Submitted Total Number	10