5IZ1
Physcomitrella patens FBPase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2015-02-17 |
Detector | MAR scanner 345 mm plate |
Wavelength(s) | 1.5418 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 74.075, 84.803, 105.748 |
Unit cell angles | 90.00, 104.59, 90.00 |
Refinement procedure
Resolution | 102.340 - 3.000 |
R-factor | 0.25711 |
Rwork | 0.254 |
R-free | 0.31508 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1d9q |
RMSD bond length | 0.010 |
RMSD bond angle | 1.399 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0073) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 104.000 |
High resolution limit [Å] | 3.000 |
Rmerge | 0.120 |
Number of reflections | 21633 |
<I/σ(I)> | 8.8 |
Completeness [%] | 88.5 |
Redundancy | 3.6 |
CC(1/2) | 0.993 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.5 | 293 | 25 % PEG 3350 0.1 M Bis-Tris |