5IYQ
Protruding domain of GII.4 human norovirus CHDC2094 in complex with HBGA type B (triglycan)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-07-27 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.97625 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 89.810, 105.930, 135.480 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.167 - 1.410 |
R-factor | 0.1277 |
Rwork | 0.126 |
R-free | 0.15590 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5iyn |
RMSD bond length | 0.007 |
RMSD bond angle | 1.235 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER (2.5.6) |
Refinement software | PHENIX |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 48.170 | 1.440 | |
High resolution limit [Å] | 1.400 | 6.260 | 1.400 |
Rmerge | 0.072 | 0.027 | 0.893 |
Number of reflections | 126435 | ||
<I/σ(I)> | 15.47 | 56.27 | 1.91 |
Completeness [%] | 99.7 | 97.9 | 98.9 |
Redundancy | 5.9 | ||
CC(1/2) | 0.999 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.6 | 291 | Sodium citrate, PEG3350 |