5IOX
Xanthomonas campestris Peroxiredoxin Q - Structure LUss
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 5.0.2 |
Synchrotron site | ALS |
Beamline | 5.0.2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-04-20 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.96486 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 34.650, 54.130, 36.610 |
Unit cell angles | 90.00, 107.72, 90.00 |
Refinement procedure
Resolution | 33.006 - 1.300 |
R-factor | 0.1834 |
Rwork | 0.182 |
R-free | 0.21350 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3gkk |
RMSD bond length | 0.009 |
RMSD bond angle | 1.296 |
Data reduction software | iMOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX (1.8.4_1496) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 34.870 | |
High resolution limit [Å] | 1.300 | 1.300 |
Number of reflections | 28974 | |
<I/σ(I)> | 8 | |
Completeness [%] | 91.4 | |
Redundancy | 6 | |
CC(1/2) | 0.314 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 300 | 1.0 M ammonium sulfate, 0.2 M sodium chloride, 0.1 M sodium cacodylate pH 6.8 |