5IOK
Crystal structure of Taf14 YEATS domain in complex with histone H3K9cr
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-10-23 |
Detector | DECTRIS PILATUS 200K |
Wavelength(s) | 1.54 |
Spacegroup name | P 65 |
Unit cell lengths | 113.095, 113.095, 26.176 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 32.648 - 2.220 |
R-factor | 0.2117 |
Rwork | 0.210 |
R-free | 0.23910 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5d7e |
RMSD bond length | 0.009 |
RMSD bond angle | 1.230 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHENIX |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 32.650 | 2.260 |
High resolution limit [Å] | 2.220 | 2.220 |
Rmerge | 0.080 | 0.330 |
Number of reflections | 9584 | |
<I/σ(I)> | 24.9 | 2.4 |
Completeness [%] | 97.1 | 72.6 |
Redundancy | 3.8 | 1.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6 | 291 | 44% PEG600 (v/v) and 0.2 M citric acid (pH 6.0) |