5ILS
Autoinhibited ETV1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL7-1 |
Synchrotron site | SSRL |
Beamline | BL7-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-02-07 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.0000 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 50.186, 50.186, 69.332 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 27.101 - 1.399 |
R-factor | 0.1577 |
Rwork | 0.157 |
R-free | 0.17830 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 1.175 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | PHASER (2.5.6) |
Refinement software | PHENIX |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 55.000 | 55.000 | 1.450 |
High resolution limit [Å] | 1.399 | 3.020 | 1.400 |
Rmerge | 0.104 | 0.063 | |
Number of reflections | 20493 | ||
<I/σ(I)> | 8.4 | ||
Completeness [%] | 100.0 | 100 | 100 |
Redundancy | 34.4 | 43.3 | 25.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 30% PEG 5000 MME, 200 mM (NH4)2SO4, 100 mM MES |