5IL6
Crystal structure of the dehydratase domain of RzxB from Pseudomonas fluorescens
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-08-30 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 1.00000 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 50.480, 105.080, 68.140 |
Unit cell angles | 90.00, 111.91, 90.00 |
Refinement procedure
Resolution | 63.217 - 1.900 |
R-factor | 0.2011 |
Rwork | 0.200 |
R-free | 0.22640 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3kg9 |
RMSD bond length | 0.003 |
RMSD bond angle | 0.658 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((1.10pre_2131: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 63.217 | 2.010 |
High resolution limit [Å] | 1.900 | 1.900 |
Rmerge | 0.067 | 0.482 |
Number of reflections | 50913 | |
<I/σ(I)> | 13.1 | 2.4 |
Completeness [%] | 98.1 | 97.3 |
Redundancy | 3.3 | 3.2 |
CC(1/2) | 0.997 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 277 | 0.1M BisTris 6.5, 0.2 M NaCl, 20% PEG6000 |