5IJI
Fragment of nitrate/nitrite sensor histidine kinase NarQ (WT) in symmetric holo state
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-09-18 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.972 |
Spacegroup name | F 2 2 2 |
Unit cell lengths | 57.702, 73.830, 235.813 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 39.400 - 1.940 |
R-factor | 0.19277 |
Rwork | 0.190 |
R-free | 0.25416 |
Structure solution method | SAD |
RMSD bond length | 0.008 |
RMSD bond angle | 1.084 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | SHELXDE |
Refinement software | REFMAC (5.8.0073) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 39.400 | 1.990 |
High resolution limit [Å] | 1.940 | 1.940 |
Rmerge | 0.083 | 0.989 |
Number of reflections | 17728 | |
<I/σ(I)> | 14.5 | 2 |
Completeness [%] | 98.9 | 98.1 |
Redundancy | 5.5 | 5.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | LIPIDIC CUBIC PHASE | 293 | in meso lipidic cubic phase crystallization |