5I5H
Ecoli global domain 245-586
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I02 |
Synchrotron site | Diamond |
Beamline | I02 |
Temperature [K] | 193 |
Detector technology | PIXEL |
Collection date | 2015-10-01 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.9798 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 56.860, 56.860, 191.810 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 47.700 - 1.650 |
R-factor | 0.17829 |
Rwork | 0.175 |
R-free | 0.23743 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5i5d |
RMSD bond length | 0.013 |
RMSD bond angle | 1.756 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0135) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.830 | 1.710 |
High resolution limit [Å] | 1.650 | 1.650 |
<I/σ(I)> | 17.8 | |
Completeness [%] | 99.6 | 99.2 |
Redundancy | 9.6 | 9.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 4.3 | 310 | 0.2 M lithium sulphate, 0.1 M sodium acetate pH 4.3 and 48% PEG400 |