5I5D
Salmonella global domain 245
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I02 |
| Synchrotron site | Diamond |
| Beamline | I02 |
| Temperature [K] | 177 |
| Detector technology | PIXEL |
| Collection date | 2015-10-01 |
| Detector | DECTRIS PILATUS 6M-F |
| Wavelength(s) | 0.9796 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 51.600, 196.090, 70.270 |
| Unit cell angles | 90.00, 95.79, 90.00 |
Refinement procedure
| Resolution | 98.040 - 1.640 |
| R-factor | 0.194 |
| Rwork | 0.192 |
| R-free | 0.22200 |
| Structure solution method | SAD |
| RMSD bond length | 0.017 |
| RMSD bond angle | 1.967 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | SHELXDE |
| Refinement software | REFMAC (5.8.0135) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 98.400 | 1.680 |
| High resolution limit [Å] | 1.640 | 1.640 |
| Rmerge | 0.200 | |
| <I/σ(I)> | 15.5 | 1.2 |
| Completeness [%] | 95.1 | 90.5 |
| Redundancy | 11.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 5.5 | 293 | in 0.1 M Bis-tris pH 5.5 and 16% PEG3350 |
