5I54
Exploring onset of lysozyme denaturation by urea - soak period 4 hours
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | BRUKER AXS MICROSTAR |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2014-08-01 |
Detector | MARRESEARCH |
Wavelength(s) | 1.5418 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 79.040, 79.040, 36.600 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 27.945 - 1.608 |
R-factor | 0.1663 |
Rwork | 0.165 |
R-free | 0.19930 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 193l |
RMSD bond length | 0.006 |
RMSD bond angle | 1.028 |
Data reduction software | iMOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 27.950 |
High resolution limit [Å] | 1.608 |
Rmerge | 0.020 |
Number of reflections | 15566 |
<I/σ(I)> | 30.22 |
Completeness [%] | 99.8 |
Redundancy | 2 |
CC(1/2) | 0.999 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 3.5 | 295 | Sodium chloride, sodium citrate |