5I4X
Exploring onset of lysozyme denaturation by urea - soak period 2 hours
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | BRUKER AXS MICROSTAR |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2013-10-20 |
Detector | MARRESEARCH |
Wavelength(s) | 1.5418 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 78.840, 78.840, 36.840 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 30.730 - 1.607 |
R-factor | 0.1793 |
Rwork | 0.178 |
R-free | 0.21270 |
RMSD bond length | 0.006 |
RMSD bond angle | 1.014 |
Data reduction software | iMOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 30.730 |
High resolution limit [Å] | 1.607 |
Rmerge | 0.036 |
Number of reflections | 15398 |
<I/σ(I)> | 14.29 |
Completeness [%] | 98.5 |
Redundancy | 1.9 |
CC(1/2) | 0.998 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 3.5 | 295 | Sodium chloride, sodium citrate |