5I4J
Dps4 from Nostoc punctiforme in complex with Zn ions
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-02-23 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.97240 |
Spacegroup name | P 63 |
Unit cell lengths | 100.920, 100.920, 144.270 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 47.631 - 2.394 |
R-factor | 0.171 |
Rwork | 0.169 |
R-free | 0.21410 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5hjf |
RMSD bond length | 0.008 |
RMSD bond angle | 1.084 |
Data scaling software | Aimless (0.5.2) |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 48.090 | 48.090 | 2.480 |
High resolution limit [Å] | 2.390 | 9.270 | 2.390 |
Rmerge | 0.123 | 0.034 | 1.681 |
Rmeas | 0.131 | ||
Rpim | 0.045 | ||
Total number of observations | 277574 | ||
Number of reflections | 32761 | ||
<I/σ(I)> | 13.9 | ||
Completeness [%] | 99.8 | 99.4 | 98.5 |
Redundancy | 8.5 | 7.9 | 8.5 |
CC(1/2) | 0.997 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 291 | 25% SOKALAN HP 66, 0.1M HEPES pH 7.0 and 0.2M NaOAc, |