5I2T
Domain characterization of the WD protein Pwp2 and their relevance in ribosome biogenesis
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 1 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 1 |
Temperature [K] | 120 |
Detector technology | PIXEL |
Collection date | 2014-03-27 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 0.978 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 70.830, 76.040, 191.350 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.398 - 2.543 |
R-factor | 0.2153 |
Rwork | 0.213 |
R-free | 0.25210 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2pbi |
RMSD bond length | 0.011 |
RMSD bond angle | 1.374 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | BALBES |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.398 | 2.680 |
High resolution limit [Å] | 2.540 | 2.540 |
Rmerge | 0.019 | |
Rpim | 0.046 | 0.651 |
Number of reflections | 34863 | 4990 |
<I/σ(I)> | 12 | 1.2 |
Completeness [%] | 99.8 | 100 |
Redundancy | 8.74 | 9 |
CC(1/2) | 0.998 | 0.536 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 293.15 | 5 % polyethylene glycol 6000, 0.1 M Magnesium Sulphate |