5HZR
Crystal structure of MtSnf2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 173 |
Detector technology | CCD |
Collection date | 2015-02-18 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.987 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 122.613, 144.266, 121.290 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 44.769 - 2.330 |
R-factor | 0.1953 |
Rwork | 0.194 |
R-free | 0.21310 |
RMSD bond length | 0.004 |
RMSD bond angle | 0.715 |
Data reduction software | HKL-2000 (V705) |
Data scaling software | HKL-2000 (V705) |
Phasing software | PHASER |
Refinement software | PHENIX ((1.10.1_2155: ???)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 62.000 |
High resolution limit [Å] | 2.300 |
Number of reflections | 41149 |
<I/σ(I)> | 24.6 |
Completeness [%] | 85.7 |
Redundancy | 5.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | EVAPORATION | 277 | ammonium sulfate, protamine, NDSB-221 |