5HWT
Crystal structure of apo-PAS1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 5C (4A) |
Synchrotron site | PAL/PLS |
Beamline | 5C (4A) |
Temperature [K] | 173 |
Detector technology | CCD |
Collection date | 2012-07-06 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 41.114, 49.314, 56.222 |
Unit cell angles | 90.00, 109.22, 90.00 |
Refinement procedure
Resolution | 25.000 - 1.700 |
R-factor | 0.1535 |
Rwork | 0.150 |
R-free | 0.22395 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.022 |
RMSD bond angle | 2.039 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.730 |
High resolution limit [Å] | 1.700 | 1.700 |
Number of reflections | 23475 | |
<I/σ(I)> | 32.94 | |
Completeness [%] | 100.0 | |
Redundancy | 7.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 294.15 | 3.0M ammonium phosphate, 0.1M Tris-HCl |