5HVX
Full length Wild-Type Open-form Sodium Channel NavMs
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 1 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-12-19 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.987 |
Spacegroup name | I 4 2 2 |
Unit cell lengths | 109.000, 109.000, 210.590 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 27.670 - 2.450 |
R-factor | 0.2087 |
Rwork | 0.207 |
R-free | 0.23320 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3rvy |
RMSD bond length | 0.010 |
RMSD bond angle | 1.000 |
Data reduction software | XDS (Oct 15, 2015) |
Data scaling software | XDS (Oct, 15, 2015) |
Phasing software | PHASER (2.5.7) |
Refinement software | BUSTER (2.10.2) |
Data quality characteristics
Outer shell | |
Low resolution limit [Å] | 2.550 |
High resolution limit [Å] | 2.450 |
Rmerge | 2.570 |
<I/σ(I)> | 1.4 |
Completeness [%] | 100 |
Redundancy | 29.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 277 | 0.05 M NaCl, 0.1 M MES buffer, pH 6.5, 37.8% v/v polyethylene glycol (PEG) 400 and 4% ethylene glycol |