5HUL
Crystal Structure of NadC Deletion Mutant in Cubic Space Group
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 22-ID |
Synchrotron site | APS |
Beamline | 22-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-02-16 |
Detector | MARMOSAIC 300 mm CCD |
Wavelength(s) | 1.0000 |
Spacegroup name | P 2 3 |
Unit cell lengths | 179.630, 179.630, 179.630 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 39.200 - 2.855 |
R-factor | 0.17169 |
Rwork | 0.170 |
R-free | 0.20518 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4kwv |
RMSD bond length | 0.018 |
RMSD bond angle | 1.712 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0135) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 2.900 |
High resolution limit [Å] | 2.850 | 2.850 |
Rmerge | 0.057 | 0.815 |
Number of reflections | 44917 | |
<I/σ(I)> | 24.1 | 2 |
Completeness [%] | 99.8 | 99.5 |
Redundancy | 4.7 | 4.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 5.5 | 293 | 1 M Ammonium Phosphate, 0.1 M Sodium citrate tribasic/ Citric acid, 0.2 M Sodium Chloride |