5HTY
Sugar kinases from Synechococcus elongatus PCC7942-D221A
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-01-22 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.97916 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 97.887, 47.206, 89.835 |
Unit cell angles | 90.00, 91.58, 90.00 |
Refinement procedure
Resolution | 32.634 - 2.815 |
R-factor | 0.2005 |
Rwork | 0.196 |
R-free | 0.24530 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.002 |
RMSD bond angle | 0.635 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | AutoSol |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.900 |
High resolution limit [Å] | 2.800 | 2.800 |
Rmerge | 0.143 | 0.468 |
Number of reflections | 10021 | |
<I/σ(I)> | 12.94 | 5.48 |
Completeness [%] | 99.9 | 100 |
Redundancy | 7 | 7.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 281 | 0.1M BIS-TRIS pH 6.5, 20% w/v Polyethylene glycol monomethyl ether 5000 |