5HT1
Structure of apo C. glabrata FKBP12
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | OTHER |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2014-03-12 |
Detector | RIGAKU RAXIS HTC |
Wavelength(s) | 1.5418 |
Spacegroup name | I 4 2 2 |
Unit cell lengths | 76.436, 76.436, 87.017 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 43.508 - 2.651 |
R-factor | 0.1984 |
Rwork | 0.191 |
R-free | 0.26270 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 1.183 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | PHENIX (1.6.4_486) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 43.508 |
High resolution limit [Å] | 2.650 |
Number of reflections | 3991 |
<I/σ(I)> | 11.8 |
Completeness [%] | 100.0 |
Redundancy | 3.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298 | PEG 4000, 0.1 M Tris 7.5 |