5HPH

Structure of TRAP1 fragment

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 19-ID
Synchrotron site	APS
Beamline	19-ID
Temperature [K]	93
Detector technology	CCD
Collection date	2015-04-26
Detector	ADSC QUANTUM 315r
Wavelength(s)	0.97929
Spacegroup name	P 21 21 21
Unit cell lengths	93.437, 104.946, 156.909
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	49.764 - 2.429
R-factor	0.1966
Rwork	0.195
R-free	0.23790
RMSD bond length	0.007
RMSD bond angle	1.035
Data reduction software	HKL-3000
Data scaling software	HKL-3000
Phasing software	PHASER
Refinement software	PHENIX (1.10_2155)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	49.764	2.470
High resolution limit [Å]	2.429	2.430
Number of reflections	58241
<I/σ(I)>	10.6
Completeness [%]	99.0	90.7
Redundancy	6.8

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	6.25	287	1.8M Ammonium Sulfate, 0.1M MES, 1% dioxane