5HLI
Structure of Disulfide formed AbfR
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-10-06 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9735 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 46.534, 51.686, 85.935 |
Unit cell angles | 90.00, 103.73, 90.00 |
Refinement procedure
Resolution | 29.037 - 2.050 |
R-factor | 0.2142 |
Rwork | 0.212 |
R-free | 0.24550 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4hbl |
RMSD bond length | 0.002 |
RMSD bond angle | 0.454 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((1.10_2155)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.120 |
High resolution limit [Å] | 2.050 | 2.050 |
Number of reflections | 24889 | |
<I/σ(I)> | 25.1 | |
Completeness [%] | 99.1 | |
Redundancy | 7.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 8% Tacsimate, 20% PEG 3350 |